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This type of mixture is distilled by extractive distillation method. First, methanoic mixture is separated by feeding the required rate of water in the extractor with the counter-current of these two liquids. Later on GC is done for methanol content in the organic layer and if it comes below the required level, it is taken for rectificaton in the column.

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Q: How do you separate mixture of methanol ethyl acetate and water?
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How do you separate mixture of methanol and ethyl acetate?

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