Using too large of a sample when determining its melting point will flaw your results since, if the sample is too large it will be harder for the sample to melt in the melting point apparatus.
We would need far more detail in order to even begin to guess why there might be any effect. The melting point of a substance is an intrinsic property; it shouldn't depend on the amount of substance being melted.
The substance will not melt appropriately or as expected, and the results could be different than they would be under normal conditions.
too small to probably observe the MP range
The melting point is an intensive property and is independent from the size of the sample.
But working with very small samples is more difficult and more errors are possible.
The melting point is not dependent from the size of the sample to be analyzed.
When work with very small samples the determination is more difficult and the result may be not so precise.
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The closer the melting point of the sample of the caffeine you have extracted, to the known melting point of pure caffeine, the more pure your sample is.
An impure sample will have a lower melting point, and will also have wider melting point range than that of a pure sample of the same substance. a sharp melting point range can also indicate a eutectic mixture
The apparatus used for determining the melting point will heat the sample at an appropriate rate. All you need to do is watch and note the point at which the sample melts, as should be demonstrated to you by your lab supervisor.
The crystalline solids have a sharp melting point say 87oC but most of the amorphous solids do not have a sharp melting point they have a range of melting say they started melting at 87oC and continue till 89oC.
The melting point is an indication of purity.
Soluble impurities (that is, impurities that are included within the crystal matrix) tend to lower the observed melting point and broaden the melting point range. Insoluble impurities have no effect on the melting point. Found from website: http://swc2.hccs.edu/pahlavan/2423L1.pdf
A lower and wider melting point range could indicate that the sample was contaminated with trace amounts of impurities.
The substance whose melting point is being observed is impure.
The closer the melting point of the sample of the caffeine you have extracted, to the known melting point of pure caffeine, the more pure your sample is.
An impure sample will have a lower melting point, and will also have wider melting point range than that of a pure sample of the same substance. a sharp melting point range can also indicate a eutectic mixture
The effect of poorly packed will decrease the melting point.
The apparatus used for determining the melting point will heat the sample at an appropriate rate. All you need to do is watch and note the point at which the sample melts, as should be demonstrated to you by your lab supervisor.
The sample is placed in a sealed capillary and heated up to the melting.
One of the easier and more reliable ways to check if a solid compound is pure after re-crystallization is to check its melting point. Impurities will always lower the melting point of a sample, and the more impure, the lower the melting point will be. By checking the melting point of your sample with a reference value from a book or reliable internet source, it can be determined exactly how impure the sample is. If perhaps your compound is unknown, and thus are unable to obtain a reference value, you could obtain melting point of the sample, and then re-crystallize a few more times, obtaining a new melting point each time, until it is unchanged by re-crystallizing. This will of course decrease your yield, but if there is little fluctuation in your series of melting points, you can be sure you have a relatively pure sample.
The crystalline solids have a sharp melting point say 87oC but most of the amorphous solids do not have a sharp melting point they have a range of melting say they started melting at 87oC and continue till 89oC.
I have just looked at several online articles about Darmstadtium and it's melting point is not listed.
Melting point of the sample & Density of the sample