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Make a solution of Sodium Hydroxide or Sodium Carbonate and do three to four solvent solvent extractions using the aqueous base and the mixture o benzoic acid and toluene. Because benzoic acid reacts with base to form the water soluble carboxylate ion, it will react and the dissolve in the aqueous solution. Upon separation of the two phases acidify the aqueous extract with dilute HCl, a white needle-like precipitate of benzoic acid will form when the solution becomes acidic. Simply filter the crystals, wash with cold water, and then recrystallize using a mixture of 50/50 water and methanol or some other suitable solvent.
Dissolve the mixture in an apolar organic solvent, such as diethyl ether, and extract the acid with the addition of NaOH. The bezoic acid with ionize and go into the aqueous solution. Separate the two layers and add HCl to the aqueous layer to precipitate the benzoic acid. Wash the remaing ether solution with water and dry it with an anhydrous salt. Filter the ether solution and then remove the ether, the solvent, in order to obtain the pure benzoin.
It is partially soluble.
You will get benzoic acid as a result. The benzoic salt will gain a Hydrogen from the HCl; thus, becoming benzoic acid, and the Cl shall remain by itself in suspension if you're mixing the two together in an aqueous solution.
Separating benzoic acid from para-nitroaniline requires a mixing stage before the separation stage. The process also requires aqueous sodium hydroxide.
Make a solution of Sodium Hydroxide or Sodium Carbonate and do three to four solvent solvent extractions using the aqueous base and the mixture o benzoic acid and toluene. Because benzoic acid reacts with base to form the water soluble carboxylate ion, it will react and the dissolve in the aqueous solution. Upon separation of the two phases acidify the aqueous extract with dilute HCl, a white needle-like precipitate of benzoic acid will form when the solution becomes acidic. Simply filter the crystals, wash with cold water, and then recrystallize using a mixture of 50/50 water and methanol or some other suitable solvent.
Dissolve the mixture in an apolar organic solvent, such as diethyl ether, and extract the acid with the addition of NaOH. The bezoic acid with ionize and go into the aqueous solution. Separate the two layers and add HCl to the aqueous layer to precipitate the benzoic acid. Wash the remaing ether solution with water and dry it with an anhydrous salt. Filter the ether solution and then remove the ether, the solvent, in order to obtain the pure benzoin.
It is partially soluble.
Any reaction occur.
Yes all organic compounds dissolve in ethers.
You will get benzoic acid as a result. The benzoic salt will gain a Hydrogen from the HCl; thus, becoming benzoic acid, and the Cl shall remain by itself in suspension if you're mixing the two together in an aqueous solution.
Separating benzoic acid from para-nitroaniline requires a mixing stage before the separation stage. The process also requires aqueous sodium hydroxide.
yes it does with heat, although it might take a super long time when heat up.
HCl + NaOH = H2O + NaCl Or, water and table salt--which will dissolve in water. Benzoic acid, C6H5COOH, will not be formed; neither of the two starting chemicals contains carbon, and benzoic acid contains a lot of it. - - - - - Benzoic acid and sodium chloride
When you're attempting to extract benzoic acid from other organic compounds, it is necessary to change its pH by adding a layer of an basic compound such as 1M NaOH so that the benzoic acid then can be separated from the organic layer within a separatory funnel. When in NaOH, the benzoic acid loses a proton and thus becomes its conjugate base (the benzoate ion). The benzoate ion is charged and thus become miscible in the aqueous layer. To extract benzoic acid (ie get it to precipitate out of solution), a strong acid such as HCl must be added to solution. After the extraction, lower the pH of the solution, and recrystalize (use ice after the recrystalization to get benzoic acid crystals to crash out).
Benzoic acid is soluble in kerosene.
Salts of the benzoic acids are called benzoates.