A water bath is only used when the material to be distilled meats two criteria. The first is that the material would deteriorate if exposed to a temperature above a certain temperature and secondly if he distillation temperature is at or below 100oC.
In the first car it is easier to control the temperature of a large volume of water because of its thermal inertia rather than control the temperature by using direct heat on a small volume of material to be distilled. In addition the water bath avoids local hot spots in the distillation vessel.
The second points obvious in that materials will not distill at temperatures below their own boiling point.
With the advent of reliable electrical heating systems water baths have been superseded with temperature controlled electrical heating systems. All the advantages of a water bath, more precise temperature control and less mess.
Because ether is highly volatile liquid and easily catch the fire (combustible) so direct heat on flame is not possible.
a water bath is then needed during distillation
with a submersion heater designed for bath tubs..
The ice water bath is an option designed to cool the distillate to speed and improve condensation, which happens in the receiver flask.
A water bath must be used while heating ethanol and acetone because the temperatures at which they can be heated might break the container they are heated in. Some metals are also heated this way.
Standard bath is taken to be 20 gallons at 8.35 pounds per gallon and 60 degrees F of heating = 10,000 BTU per bath in round numbers, assuming 100% efficiency water heating.
no, it is more safe to use water bath :)
The advantage of using evaporation by water bath over a direct heating method is when heating directly, for example, with a Bunsen flame - the substance in the boling tube may decompose upon such an accelerated heating because of variations in the intensity of the flame and then may be scorched, while a water bath provides a constant heating of the subsatnce by distributing heat to the boiling tube equally throughout, so that the substance cautiously gets heated until a fixed point (be it the melting point or boiling point) is reached.
Heating it on a flame will cause possibly dangerous vapour. Hot water avoids this.
For slow heating with the maximum control, test tubes are heated in a water bath rather than in a flame. This can only heat the tube to the boiling point of water, 100°C or 212 °F.
Hypertonic
Hypertonic