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Tempering would be a fairly easy one. Find some fairly high carbon steel (mild steel won't work, and avoid the alloy ones unless you know they'll behave properly), Heat it red hot, and allow it to cool at differing rates (air cool one, quench one, stuff one into pearlite insulator to cool, etc) then do some strength tests on the cooled samples. Applies to almost any hot manufactured part. Also shows up in unexpected places, eg welding a heat treated part may mean that the whole welded assembly needs to be heat treated again or it will crack.

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Q: What can you do for mini project in thermal engineering relating to a manufacturing process?
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