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How do you make dimethyl titanocene?

Updated: 5/25/2024
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11y ago

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Titanocene dichloride &methyl grignard in toluene medium at 5'c

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11y ago
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2mo ago

Dimethyl titanocene can be synthesized by reacting titanocene dichloride with lithium aluminum hydride and methyl iodide in anhydrous conditions. The reaction typically takes place in a nonpolar solvent like diethyl ether and requires careful handling due to the reactivity of the reagents involved. Purification methods such as column chromatography may be employed to isolate the desired product.

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