From benzenesulfonic acid sodium salt and phosphorous pentachloride (PCl5) or phosphoroxychloride (POCl3).
Details in: Roger Adams, C. S. Marvel, H. T. Clarke, G. S. Babcock, and T. F. Murra, Org. Synth. Coll. Vol. 1 p. 84.
http://www.orgsyn.org/orgsyn/pdfs/CV1P0084.pdf
no it is not. it is a sulfonyl chloride
Sodium chloride is not soluble in benzene.
The full form of BHC is BENZENE HEXA CHLORIDE.
Methane could be used used for preparation of toluene but not directly. First, methane is reacted with chlorine to give chloromethane and that chloromethane is reacted with AlCl3 to form CH3+ and AlCl4- . This is reacted with Benzene(C6H6). This yields toluene as CH3+ replaces a hydrogen from Benzene.
Benzene is nonpolar, so its molecules do not have any strong attraction to sodium chloride, which is ionic.
vinylogous?
Methylene chloride and benzene are immiscible in each other. They have different chemical properties that prevent them from forming a homogeneous mixture when combined.
To synthesize acetophenone from benzene, you just need to add the aldehyde to the benzene ring. This can be done via a Friedel-Crafts acylation. The reagents are an acid chloride (acetyl chloride in this case) and AlCl3 (stoichiometric).
p-acetaminobenzenesulfonyl chloride may degrade when left to stand for some hours due to hydrolysis of the sulfonyl chloride group. This could result in the formation of byproducts and a decrease in the purity of the compound. It is recommended to store and handle the compound under appropriate conditions to prevent degradation.
The reaction of chlorobenzene with sulfuric acid and heat would likely result in electrophilic aromatic substitution, with the sulfuric acid acting as a catalyst. This reaction may lead to the formation of benzene sulfonic acid as the major product. Heating the reaction mixture helps drive the reaction forward by increasing the kinetic energy of the molecules involved.
*hinsberg reagent -Benzene sulphonyl chloride( C6H5SO2Cl) with primary amine gives n-ethylbenzenesulfonamide which is soluble in alkali *hinsberg reagent with 2 amine forms n,n-diethyl benzene sulphonamide which is insoluble in alkali *3 amine do not show this rxn
Yes, benzene-methanol can react with chlorides, particularly in the presence of a catalyst or under specific conditions. The reaction typically involves the substitution of a hydrogen atom on the benzene ring or the methanol group, leading to the formation of alkylated or chlorinated benzene derivatives. The reactivity largely depends on the type of chloride used and the reaction conditions.