A micro balance is an instrument capable of making precise measurements of weight of objects of relatively small mass: of the order of a million parts of a gram. In comparison, a standard analytical-balanceis 100 times less sensitive; i.e. it is limited in precision to 0.1 milligrams. Micro balances are generally used in a laboratory as standalone instruments but are also incorporated into other instruments, such asnermogravimetry, and sorption/desorption systems, and surface property instruments.
Instrument
Wooden block (4 cm x 4 cm x 2 cm)
Wooden strip (15 cm x 2 cm, for example, a medical tongue depressor)
Elastic bands (5 cm), 2
Needle (fine)
Metal screw (1.2 cm)
Aluminum support (see Technical notes)
Drinking straw (waxed paper or plastic)
Graph paper - at least 100 sheets
Scissors
Sensitive laboratory balance
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As part of the reviewing process, the experiments on this website have been checked for health and safety. In particular, we have attempted to ensure that:
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Geysers do not make energy.
Things that make light
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With a microbalance.
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Ronald Verne Hill has written: 'The design and analysis of a microbalance system' -- subject(s): Microbalances
graduated cylinder c: --------------------------------------------------------------------------------- A mass is determined with different types of balances, from a microbalance to a truck weighing machine. The SI unit of mass is the kilogram (kg).
It depends on how you use it. If you are just looking for a small differential weight then calibration is not as critical. If you are looking for the actual weight of an item then calibration should be done more regularly. Having a professional check it once or twice a year is a good idea, and run periodic checks of your own. Daily in critical applications, less frequent if not as critical.
a Fix the wooden strip to the wood block as illustrated using the elastic bands twisted twice round the block.b Insert the small metal screw in one end of the drinking straw.c Cut away the other end of the straw with scissors so that it acts both as a pointer and as a little scoop into which items to be weighed can be placed.d Find the approximate centre of gravity by balancing the straw on the needle. Then push the needle through the straw to act as the rolling axle. It should be put through just above the long axis of the straw.e Use standard masses (paper squares) to calibrate the microbalance. Mark the zero position of the pointer high up on the vertical scale. Put the 1 mm2 weight into the scoop and mark the pointer position. Continue adding weights until a uniform scale is constructed.f Other things that might be weighed include a flake of mica, a small piece of thread, a small piece of iron wire before and after rusting, a drop of olive oil, and the loss in mass as a drop of ether evaporates.g Order of magnitude calculations can be fun. Once the mass of a grain of sand is known estimate and then measure the mass of a beaker of sand.
1. Weight 175,32 mg ultrapure NaCl with a microbalance. 2. Transfer quantitatively NaCl in a 1 L clean volumetric flask. 3. Add 950 mL demineralized water. 4. Put the flask in a thermostat at 20 0C and maintain for 30 min. 5. Add demineralized water to the mark. 6. Stir the flask. 7. Transfer the solution in a clean and dry bottle of glass, PE, PP. 8. Add the necessary label: date, name of the solution, operator.
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- Dry potassium dichromate (standard certified quality, from NIST - SRM 136f or from another supplier), using a platinum dish or crucible. - Follow the mode of drying (generally 1 hour at 120 0C in an oven) indicated by the supplier. Place the potassium dichromate in an exsicator. - Prepare a volume of demineralized or distilled water - Weight 73,546 25 g potassium dichromate in a platinum dish calcined to a constant weight; apply a correction for the flotability of the air and the purity of the dichromate. Use a metrologically checked microbalance. - Place carefully the potassium dichromate in a 1 000 mL volumetric flask, dried and washed - Add about 900 mL water - Place the volumetric flask in a thermostat at 20 0C; after approx. 30 min add the water exactly to the mark. - Stirr the content of the volumetric flask; place a clear label on the flask (concentration, material, date of preparation, operator's name).
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To Make It Make Sense was created in 2009.