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Gas chromatography (GC) and gas chromatography-mass spectrometry (GC-MS)

At present, GC and GC-MS have become the most commonly used qualitative and quantitative detection methods of silicone rubber for volatile cyclosiloxane in food contact silicone rubber.

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Zetarmold

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Test methods for silicone rubber?

The detection properties of silicone rubber can be said to be between organic and inorganic substances. It contains a variety of small molecules and polymers, and the environment of food-contact silicone rubber is complex and diverse. The food itself can be divided into water, alcohol, acid, and oil. Such steamer mats, baking mats, etc., need to be used for a long time under high temperature and high humidity environments, so it is difficult to analyze. The analysis and detection of toxic substances in silicone rubber can be roughly divided into two ways. One is to directly and qualitatively detect the presence of toxic substances in silicone rubber materials. For example, gas chromatography-mass spectrometry can take advantage of the high efficiency of gas chromatography and the strong qualitative power of mass spectrometry to directly detect toxic substances such as cyclosiloxane migrating from silicone rubber products. Secondly, by analyzing the molecular structure changes of silicone rubber before and after aging, the aging mechanism can be inferred to determine the possibly toxic substances. At present, infrared spectroscopy, nuclear magnetic resonance, and other analytical methods are usually used to infer the aging mechanism of silicone rubber, simple and fast. I. Silicone rubber test method Gas chromatography (GC) and gas chromatography-mass spectrometry (GC-MS) At present, GC and GC-MS have become the most commonly used qualitative and quantitative detection methods of silicone rubber for volatile cyclosiloxane in food contact silicone rubber. The method is suitable for the separation and analysis of complex volatile components with strong chromatographic separation ability and high mass spectrometry resolution. With high separation efficiency and high sensitivity, GC-MS technology is widely used in food safety, environmental pollution, food and pesticide residue detection, and other fields. In the process of thermal degradation of siloxane rubber, small molecules of circular siloxane were produced, and the low molecular weight circular siloxane migrated from silicone rubber products for food contact was detected by GC-MS, and methyl cyclosiloxane had the lowest single component, the detection amount was 50mg/kg. On October 1, 2012, the implementation of “Determination of Volatile methylcyclosiloxane residues in silicone rubber” (GB/T 28112-2011) explained in detail the principle of determining the residual volatile cyclosiloxane (D4~D10) content in silicone rubber by gas chromatography. Silicone rubber detection method Fourier transform infrared spectroscopy (FTIR) and nuclear magnetic resonance (NMR) FTIR and NMR are important tools for analyzing the organic structure of silicone rubber materials. Among them, infrared spectroscopy is an important method to identify the composition of silicone rubber materials. NMR can obtain information about its molecular skeleton structure, and they are widely used in the study of the microstructure of silicone rubber. Infrared spectroscopy does not require sample pretreatment, is low cost has high efficiency and has no pollution, so it is widely used in the food industry. At present, the NMR detection of silicone rubber is mainly used in the medical field, industrial field, and biological field. Although there are few reports on the detection of migratory toxic substances in silicone rubber that come into contact with food, foreign scholars have used nuclear magnetic resonance. Spectroscopic detection of cyclosiloxanes with low detection limits and very specific qualitative and quantitative information.


Can you glue fabric with rubber cement?

A general rule when talking about silicone rubber: Nothing sticks to silicone -- except silicone. As long as you have a silicone based adhesive, you should be able to stick anything the silicone. Warning: if you are using any type of silicone adhesive, it will bond to fabric permanently, so make sure you aren't wearing any nice clothes. Latex or nitrile gloves are also recommended when handling silicone adhesive.


How do you smoothen rubber?

To smoothen rubber, you can use fine sandpaper or a file to gently buff the surface, removing any imperfections. For a more polished finish, apply a rubber conditioner or silicone spray, which can enhance the surface texture and provide a protective layer. Additionally, heat can be applied cautiously using a heat gun to soften the rubber, allowing for easier smoothing. Always test on a small area first to avoid damage.


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To effectively remove dried silicone, you can use a silicone remover or solvent to soften the silicone, then scrape it off with a putty knife or scraper. You can also try using rubbing alcohol or vinegar to break down the silicone. Be sure to follow safety precautions and test a small area first to avoid damaging the surface.


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A fair test is the goal of many an enquiry. A test should not be biassed by the selection of subject, by the test method itself, nor by the method of analysis.


How can I effectively remove silicone from glass surfaces?

To effectively remove silicone from glass surfaces, you can use a razor blade or scraper to carefully scrape off the silicone residue. Alternatively, you can use a silicone remover solution or rubbing alcohol to dissolve and wipe away the silicone. Be sure to follow safety precautions and test a small area first to avoid damaging the glass surface.


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