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Check the book Macroscale and Microscale by Williamson and Masters. Go to the chapter entitled Nitration of Methyl Benzoate. The synthesis of 3-nitrobenzaldehyde/3-nitrobenzoic acid has the same procedure.

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4d ago

3-nitrobenzaldehyde can be synthesized by nitration of benzaldehyde with nitric acid in the presence of a catalyst such as sulfuric acid. The reaction is typically carried out under controlled conditions to avoid excessive nitration. After the reaction, purification techniques such as recrystallization can be used to isolate the final product.

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Q: What is the procedure for synthesis of 3-nitrobenzaldehyde?
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