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Take p-bromoacetanilide in a round bottom flask n reflux it on a water bath using ethanol and HCl. Reflux it for around 30 minutes. Cool it in an ice bath and neutralise with 20% NaOH. Filter the separated p-bromoaniline.

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14y ago
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12y ago

When phenol is heated with acetic anhydride crystals of phenyl benzoate are formed which are filtered off washed with water and dried.


There are a number of different ways. Reacting benzoyl chloride with phenol is a good route.
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14y ago

Synthesis of benzanilide from benzophenone?

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12y ago

C6H5-NH2 + C6H5-Cl-C=O-CH3------------>benzanilide + HCL

NAOH

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14y ago

see this link:

http://www.orgsyn.org/orgsyn/orgsyn/prepContent.asp?prep=CV1P0082

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14y ago

Benzoic acid may be prepared by oxidation of benzaldehyde,

C6H5-CHO + KMnO4 = C6H5-COOH

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10y ago

It isn't. Chlorobenzene is prepared by chlorinating benzene.

The resulting compound can be nitrated to produce nitrochlorobenzene, which is then hydrogenated to produce chloroaniline.

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Q: Preparation of p-bromoaniline from p-bromoacetanilide
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