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1) It will have a boiling point that is lower than the melting point of the solid being recrystallized; 2) The compound will be soluble in the boiling solvent but have poor solubility in the same solvent after cooling; 3) Small amounts of impurities present in the crude solid will be soluble in the chosen solvent at any temperature
What else can I help you with?
When doing a solvent pair recrystallization which of the following pairs will work ethanol and water methylene chloride and water dimethylformamide and diethyl ether?
Ethanol and water is a suitable solvent pair for recrystallization. Methylene chloride and water, as well as dimethylformamide and diethyl ether, are not typically used together as solvent pairs for recrystallization due to their different chemical properties and solubility characteristics.
Explain why during the recrystallization of p-dibromobenzene the turbidity of the hot solution was used as an indicator for the ratio of ethanol to water used?
ethanol alone is not a good solvent for this substance recrystallization and the compound has a very low solubility in hot or cold water.so ethanol and water are mixed together as solvent for crystallization of p-dibromobenzene that is soluble in the hot solvent mixed.so the turbidity of the hot solution shows the good mixture of ethanol and water as solvent.
Is Chloroform a good solvent for recrystallization in acetanilide?
Chloroform is not a commonly used solvent for recrystallization of acetanilide. It is more commonly used for dissolving non-polar or slightly polar compounds. In the case of acetanilide, solvents such as ethanol or ethyl acetate are often preferred for recrystallization.
What are the characteristics that identify a good recrystallization solvent?
A good recrystallization solvent should have the following characteristics: high solubility for the compound being purified at high temperatures, low solubility at low temperatures to allow for crystal formation, non-reactive with the compound, and easily removable from the crystals after recrystallization.
Will acetanilide dissolve in hot heptane?
Yes, acetanilide is likely to dissolve in hot heptane due to their similar polarities. Heptane is a nonpolar solvent which can dissolve nonpolar or slightly polar compounds like acetanilide. Heating the solvent can increase its ability to dissolve the compound.
What are the desirable properties of a recrystallization solvent?
One property that a solvent should have to be well suited for recrystallization of a particular compound is high solubility. It should also readily dissolve the organic compound at high temperature and precipitate the compound at low temperature.
When doing a solvent pair recrystallization which of the following pairs will work ethanol and water methylene chloride and water dimethylformamide and diethyl ether?
Ethanol and water is a suitable solvent pair for recrystallization. Methylene chloride and water, as well as dimethylformamide and diethyl ether, are not typically used together as solvent pairs for recrystallization due to their different chemical properties and solubility characteristics.
How do you prevent immature recrystallization?
To prevent immature recrystallization, ensure that the solvent is added slowly to the solution during recrystallization, use a minimal amount of solvent, and employ a suitable solvent system based on the solubility of the compound. Additionally, controlling the rate of cooling during recrystallization can help prevent premature crystallization of impurities.
Explain why during the recrystallization of p-dibromobenzene the turbidity of the hot solution was used as an indicator for the ratio of ethanol to water used?
ethanol alone is not a good solvent for this substance recrystallization and the compound has a very low solubility in hot or cold water.so ethanol and water are mixed together as solvent for crystallization of p-dibromobenzene that is soluble in the hot solvent mixed.so the turbidity of the hot solution shows the good mixture of ethanol and water as solvent.
Explain why crystallisation would not be suitable for purifying water?
An ideal crystallization solvent should be unreactive, inexpensive, and have low toxicity.It is also important that the solvent have relatively low boiling point as its best if the solvent readily evaporate from the solid once recovered.For most organic compounds, water is not a good recrystallization solvent.
What is the recyrstallization solvent for benzocaine?
Common recrystallization solvents for benzocaine include ethanol and ethyl acetate. The choice of solvent will depend on the solubility of benzocaine in the solvent at different temperatures. It is recommended to perform a solubility test to determine the most suitable solvent for recrystallization.
Is Chloroform a good solvent for recrystallization in acetanilide?
Chloroform is not a commonly used solvent for recrystallization of acetanilide. It is more commonly used for dissolving non-polar or slightly polar compounds. In the case of acetanilide, solvents such as ethanol or ethyl acetate are often preferred for recrystallization.
What are the characteristics that identify a good recrystallization solvent?
A good recrystallization solvent should have the following characteristics: high solubility for the compound being purified at high temperatures, low solubility at low temperatures to allow for crystal formation, non-reactive with the compound, and easily removable from the crystals after recrystallization.
Will acetanilide dissolve in hot heptane?
Yes, acetanilide is likely to dissolve in hot heptane due to their similar polarities. Heptane is a nonpolar solvent which can dissolve nonpolar or slightly polar compounds like acetanilide. Heating the solvent can increase its ability to dissolve the compound.
What is the disadvantage of having excess solvent during recrystallization?
Having excess solvent during recrystallization can result in a lower concentration of the desired compound in the final crystal product. This can reduce the purity of the compound and make it more difficult to separate from impurities. Additionally, excess solvent can increase the time required for the recrystallization process to complete.
Why is the product formed from recrystallization sometimes contaminated with impurities?
The product formed from recrystallization can be contaminated with impurities if they are more soluble in the solvent used for recrystallization compared to the desired compound. In this case, the impurities will remain in the solution while the desired compound forms crystals, leading to impurity inclusion in the final product. Proper choice of solvent and recrystallization conditions can help minimize impurity contamination.
What is a good solvent for recrystallization of sodium benzoate?
A good solvent for recrystallization of sodium benzoate is water, as sodium benzoate is highly soluble in water. Additionally, ethanol can also be used as a co-solvent to enhance solubility and increase the purity of the recrystallized product.
