0
Usually, solvents at lower temperature can dissolve lower amount of crystals than solvents at higher temperatures.
For eg. if impurity is salt then you are better off washing it at a lower temperature as salts have a good solubility even at lower temperatures and as you raise temperature your crystals will start dissolving in the warm solvent.
What else can I help you with?
What are the disadvantages of crystallization over evaporation to dryness?
Crystallization may require more time and effort to obtain pure crystals compared to evaporation to dryness. Crystallization can also lead to loss of product if the crystals are difficult to separate from the mother liquor. Additionally, some compounds may not readily form crystals, making crystallization less effective in those cases compared to evaporation to dryness.
The purging of impurities from a compound by crystallization?
Yes, it is. You dissolve your substance in the smallest amount possible of something suitable, hot - often ethanol. Then you cool it down and the substance should solidify. You filter to keep the solid and get rid of the impurities in the liquid. The trick is choosing the solvent wisely so that you get a good solubility when hot and not when cold.
Assuming that charcoal and sugar are the main impurities present in a sample of crude acetanilide explain how recrystallization from water would remove each..?
Recrystallization from water would remove charcoal impurities by dissolving the acetanilide in hot water, as charcoal is insoluble in water. The sugar impurities would also be removed because they are more soluble in hot water than in cold water, so they would remain dissolved during the recrystallization process and be removed in the mother liquor.
How can you produce potassium gold cyanide give detail?
how I make PGC : 1. Make aquaregia (75% HCL + 25% HNO3) from high grade chemical. 2. Introduce the Gold (24 kt) in bulk or small piece in warm aquaregia for fast soluble. (gold : aquaregia is about 1 : 5 weight). 3. Heat the solution, don't exceed 85 degree Celcius. 4. A long heating introduce excess HCL. 5. Heat and evaporated until you got a concentrate like syrup that is Gold Chloride. 6. Gold chloride will become cristall when you cool the syrup. 7. Introduce a little water to disolve the gold chloride. 8. Make amonia solution of 30 ml Amonia in 100 ml water cocentration. (use high grade amonia). 9. Pour the amonia slowly to Gold Chloride until Ph=8. You will get the precipitate that call Gold Fulminating. Be carefull with the Fulminating, It should not to dry because it is Highly Explosive Danger ! 10. Wash the Precipitate to remove excess amonia. Wash several time until PH reach near 7. 11. Make another concentrate Potasium Cyanide solution (KCN). 12. Pour the KCN to Fulminating Gold slowly with agitation until all the fulminating disolve. You Got a solution name Mother Liquor. 13. Heat the Mother Liquor, my experience not over 65 degree celcius. Evaporate amonia from mother liquor until no amonia smell anymore. 14. Cristallize the PGC by continue evaporation. Vacum will be very helpfull. You don't need to evaporate all the mother liquor. Until you evaporate about 75% volume stop the process. Collect the PGC and keep the mother liquor. Dry the PGC by vacum. Mother liquor still can be use in the next production by mixed it with the next Fulminating. 15. Do the all the process in very good ventilation. Good luck.
Some reasons why crystallization process will not give 100 percent recovery?
Some reasons why crystallization process will not give 100 percent recovery include impurities present in the solution which may remain in the mother liquor, incomplete dissolution of the solute, losses during filtration or other separation steps, and solute degradation or decomposition during the process.
What is mother liquor in crystallization?
Mother liquor is a deprecated term from older chemistry texts that refers to the solution that remains after crystallization occurs and the crystals are removed.
What are the disadvantages of crystallization over evaporation to dryness?
Crystallization may require more time and effort to obtain pure crystals compared to evaporation to dryness. Crystallization can also lead to loss of product if the crystals are difficult to separate from the mother liquor. Additionally, some compounds may not readily form crystals, making crystallization less effective in those cases compared to evaporation to dryness.
What relationship to you is your mother's cousin's daughter?
Your mother's first cousin is your first cousin once removed. Your mother's second cousin is your second cousin once removed. If you are talking about your mother's first cousin once removed, you may be first cousins twice removed or second cousins, depending on the specifics.
What relation is mother's niece's children to her?
Your mother's nieces' children are your mother's grand nephews or grand nieces. They are your first cousins, once removed.
Is your mother's cousin considered your aunt?
No, your mother's first cousin is your first cousin once removed. Her second cousin is your second cousin once removed. Your mother's sister is your aunt.
Can a child be removed from Mother for indiscretions?
Yes.
How is your mom's cousin related to you?
Your mother's first cousin is your first cousin, once removed. Your mother's second cousin is your second cousin, once removed.
Can you give your 7 month puppy watered down milk?
It is not reccomended to give any dog milk, other than dog milk from its mother. There is too much calcium in it, which can lead to bladder stones or crystals which can be very painful, and possibly have to be surgically removed.
What is your mother's cousin's relation to you?
Your mother's first cousin is your first cousin, once removed
What relation to me is my mother's mother's brother's son?
He would be your first cousin once removed.
What is your mother's first cousin's once removed husband to you?
The husband of your mother's first cousin, once removed, is not related to you as you do not share a common ancestor. In some cases, your mother's first cousin once removed is your second cousin. so you would refer to the husband as "my second cousin's husband." In other cases, your mother's first cousin, once removed, is your first cousin, twice removed. It might be easier to refer to that husband as "my gransmother's first cousin's husband."
How are you relatived to your moms second cousin once removed?
Your mother's second cousin twice removed is either your third cousin once removed or your second cousin three times removed. Which it is depends on whether the second cousin twice removed is the grandchild of your mother's second cousin or the grandparent of her fourth cousin.
