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firstly, take 1ml of sodium silicate and add 99ml of water. titrate it with 0.5N HCl and use 1 drop phenophthalein as indicator. the amount of HCl used is converted to gram by using the density and molecular weight calculations.

1.177gm of HCl used for 1 gm of sodium oxide, calculate by multiplying your HCl used for your sodium oxide.

now take 10ml of silicate and weigh it in grams and heat it at 180 degrees celsius for 2 hours to get solid content (water evaporated)

deduct the value of sodium oxide from total solid content obtained.

this is the value of silica in your sodium silicate.

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Q: Methods to determine silica content in sodium silicate?
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