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If you mean the elements that are gases at standard temperature and pressure the the first four gases to be discovered are:

hydrogen (H) was discovered by Henry Cavendish in 1766;

nitrogen (N) was discovered by Daniel Rutherford in 1772;

oxygen (O) was discovered by Joseph Priestly in 1774; and

chlorine (Cl) was discovered by Carl Wilhelm Scheele in 1774.

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