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7g Anthranilic Acid, 5ml o-Toluidine and 4 ml glacial acetic acid was mixed in a round-bottomed flask. To this mixture was slowly added 40-50 grams of polyphosphoric acid, and the mixture was heated during 20-30 minutes to 140-160°C. After this, the mixture was heated to 180°C for 10 minutes, then cooled and poured in 150-200ml water, and neutralized with 20% Na2CO3 solution. Methanol was added until a lasting turbidity became present in the solution, and after one hour, the free base Methaqualone precipitated, mp 111-113°C, and was once more recrystallized in this fashion, mp 113-115°C. Yield 55%.
What else can I help you with?
What is a sentence using the word synthesize?
Scientists have learned how to synthesize new elements. The ability to synthesize human tissues is a great medical advance.
How do you use the word synthesize in a sentence?
Chemists soon found a way to synthesize the rubber needed for the war effort.With the advent of modern computers, it is possible to digitally synthesize most sounds, even human voices.
Can you provide some organic chemistry 1 synthesis practice problems?
Here are some organic chemistry 1 synthesis practice problems: Synthesize 2-methylpentane from 1-pentene. Synthesize 2-bromopropane from propene. Synthesize 2-methyl-2-butanol from 2-methyl-2-butene. Synthesize 1,2-dibromopropane from propene. Synthesize 2,3-dimethylbutane from 2-methyl-2-butene. These problems will help you practice your skills in organic synthesis.
Can you provide some organic chemistry synthesis practice problems for Orgo 1 students?
Here are some organic chemistry synthesis practice problems for Orgo 1 students: Synthesize 2-methylpentane from 1-pentene. Synthesize 2-bromopropane from propene. Synthesize 2,4-dimethylhexane from 1-hexene. Synthesize 2-chloro-2-methylbutane from 2-methyl-1-butene. Synthesize 3-ethyl-2-methylhexane from 1-hexyne. These problems will help students practice their skills in planning and executing organic synthesis reactions.
Why would scientists synthesize something that already exists?
Scientists may synthesize something that already exists in order to better understand its properties, to create a purer form, or to make improvements to the existing substance. It can also be done to produce the substance in larger quantities or for specific applications.
Is methaqualone still prescribed for sleep?
no
Where can you buy methaqualone?
Mexician pharmices
What type of drug is methaqualone?
hihi i have no idea
How do you make methaqualone?
http://www.erowid.org/archive/rhodium/chemistry/quaalude.cheapskate.htmlGo there step by step guide
What does the nitrogen synthesize in plants?
nitrogen helps synthesize protein.
Do nucleolus synthesize ribosomes?
Yes they synthesize them. Separate parts are produced
What has the author Margaret Elizabeth Williams written?
Margaret Elizabeth Williams has written: 'Biopharmaceutical studies on methaqualone'
What is the definition of synthesize?
To combine by synthesis; to unite., To produce by synthesis; as, to synthesize albumin.
What is a sentence using the word synthesize?
Scientists have learned how to synthesize new elements. The ability to synthesize human tissues is a great medical advance.
What does it mean to synthesize ideas?
To synthesize ideas is to create new ideas from existing ones.
Can a plant cell synthesize a new chloroplasts?
Yes it can synthesize chloroplasts. they are much needed.
What monsters do you need to synthesize the missing lynx on dqm 2?
You must scout it. You can't synthesize it!
