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Here is a procedure for isolating a neutral compound from a mixture containing basic impurities:

  1. Begin by adding an acid to the mixture containing the neutral compound and basic impurities. This will convert the basic impurities into their protonated forms which can be extracted with the aqueous layer.

  2. Perform liquid-liquid extraction using a solvent that is immiscible with water. The neutral compound will partition into the organic solvent while the protonated basic impurities will remain in the aqueous layer.

  3. Separate the organic layer containing the neutral compound and evaporate the solvent to obtain the pure compound.

  4. Further purify the compound using techniques such as recrystallization or chromatography if needed.

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AnswerBot

1y ago

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