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Which instrument is most often used to measure acid volume before a titration begins?
A volumetric flask is usually used; it is the most accurate instrument for liquid volume measure, and since titrations are highly quantitative, it's the best choice.
Why is it important to clean a burette?
It is important to remove the filter funnel before adjusting the level of the burette so as to prevent the residual drops of the reagent from dripping into the burette. Which can lead to inaccurate volume readings.
Why does the pH change rapidly at the equivalence point of a titration?
The equivalence point represents a region where the amount of acid to base (or base to acid) concentration is equal. Before the equivalence point there is a greater amount of acid (or base, depending on the titration). After the titration there is a greater amount of base (or acid). This reverse in dominance results in a dramatic change in pH.
What is The process of adding a known amount of solution of known concentration to determine the concentration of another solution is called?
titration is the best method to determine the unknown concentration of the unknown. if ur known is a solid then you would have to used distilled water to ensure it is submerged before you titrate.
Why KmnO4 is used as self indicator?
As we all know that the potassium permanganate (KMnO4) is the dark purple color solution ...and in titration it become colorless ....so when the titration is completed ...and the other single drop of KMnO4 solution produce pinkish colour in a beaker ...which indicate that the reaction was completed just a single drop before .. we use indicator in a a reaction in order to indicate ...but we dont used indicator in titration with KMnO4 because it also indicate us by changing its color ...colorless to pink
What are the precaution steps in during titration?
Ensure that all glassware and equipment are clean and dry before starting the titration. Use a calibrated burette to accurately measure and deliver the titrant into the analyte solution. Perform a rough titration to determine an approximate endpoint before carrying out the actual titration. Record the volume of titrant added at the endpoint accurately to calculate the concentration of the analyte.
Why is the outside of the burette wiped with paper towel before titration?
The outside of the burette is wiped with a paper towel before titration to ensure that any liquid droplets on the outer surface do not affect the accuracy of the titration by inadvertently entering the solution being titrated. This helps to prevent contamination and ensure precise measurements are obtained during the titration process.
What happens if the tip of the burette is not filled before the titration begins?
If the tip of the burette is not filled before the titration begins, inaccurate volume readings may result due to the introduction of air bubbles into the liquid being dispensed. This can lead to imprecise titration results and affect the accuracy of the experiment.
How would the results of a titration be affected if the burette is not rinsed with a titrant?
If the burette is not rinsed with the titrant before starting the titration, there may be leftover residue from the previous solution which could lead to contamination and affect the accuracy of the results. It could also cause inconsistent readings as there may be mixing of the two solutions resulting in erroneous titration endpoints.
What is the trial titration?
A trial titration is carried out before the actual titrations and is not recorded. It is carried out by adding increments of several milliliters from the reactant in burette. It helps to give a rough estimation to the end point.
Why ist necessary to rinse the clean burette before filling it with the unstandardised sodium hydroxide solution?
It is important to rinse the clean burette to remove any residual contaminants or impurities that could affect the accuracy of the titration results. Additionally, rinsing helps to ensure that the burette is properly conditioned for the new solution being used. This step helps to avoid any potential errors or inaccuracies in the titration process.
Would it matter if droplets of distilled water were left in the burette when it was filled with sodium hydroxide?
Yes, it would matter because any residual water in the burette could potentially dilute the sodium hydroxide solution, leading to inaccurate measurements or titration results. It is important to ensure the burette is completely dry before filling it with the sodium hydroxide solution to avoid any potential errors.
What are the factors to be considered while using the burette?
Some factors to consider when using a burette include ensuring it is clean and dry, accurately reading the volume markings at eye level, properly filling and dispensing the liquid to prevent air bubbles, and taking the initial volume reading before starting the titration.
Why do you need to rinse your a buret before titration?
To wash out any trace chemicals. These trace chemicals coul affect the titration result. If the burette is clean ( from the lab. store), it will have been through the stores washing machine, so there may be trace solvents left behind.
Why do you need to remove the funnel before carrying out the titration?
Removing the funnel before titration ensures that all the liquid being added comes into direct contact with the solution being titrated. This helps to ensure accurate measurements and avoids any potential contamination from the funnel.
Why is it necessary to rinse the burette with sodium hydroxide before you completely fill it up?
Before a burette is used, it needs to be cleaned. During the cleaning process, usually, water is introduced into the burette. Be the water clean or not, if the burette is then used without rinsing it with the solution that it is going to be filled with, the result of that analytical exercise will not be precise and accurate. The reason is that water residue in the burette would dillute the solution when it's filled in the burette which would make it impossible to determine the exact concentration of the solution moved by the burette. By rinsing and re-rinsing the burette several times with the solution it is going to be filled with, residue water from the cleaning process would be successfully removed from the burette as are other leftover substances from the cleaning process. This practice is quite important as basic analytical technique.
What happens when a drop remains hanging from the tip of the burette after the solution has been added to the flask?
If a drop remains hanging from the tip of the burette after the solution has been added to the flask, it could lead to inaccuracies in the volume measurement since that drop has not been delivered into the flask. To ensure accurate measurements, it is important to wait until the drop completely detaches from the tip before stopping the titration.
