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Please refer ASTM D 3171 Procedure B, where you have to digest the matrix i.e. resin in Sulphuric acid and Hydrogen peroxide and remaining will be carbon.

With burnoff method there is Approx 5 % loss in carbon @ 500ºC, so it is not a good method for CFRP.

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Q: How do you separate carbon fiber from PES resin to measure fiber length We have tried to use a muffle furnact at 800C and it seems to burn off the carbon fibers?
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