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There's a bit of confusion here between the terms 'negate' and 'destroy'. MST is a destruction card, it cannot negate the effect of an activated card. If Polymerization is activated, chaining a destruction card to it like MST won't do anything. Polymerization's card may go to the graveyard earlier than normal but the effect will still resolve. Likewise chaining a second MST will just destroy the first MST's card, but the first MST will still resolve, though as above there is no need to 'save' Polymerization since it's going to resolve properly anyway.

To stop Polymerization from resolving, you must use a negation card like Magic Jammer. That will stop the effect from ever happening.

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Q: If you have a mst facedown and then you play a spell card like polymerization then your opponent uses mst to destroy polymerization can you use your mst to destroy their mst and save polymerization?
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