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The major disadvantage of using ether as an extracting solvent is that it is very flammable. It also oxidizes into an explosive in some cases, is an anesthetic, and is very vapor dense (meaning it will fall to the floor and move around there).

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9y ago
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13y ago

The main disadvantage of using ether is safety. Ether is explosive, highly flammable, and spontaneously forms peroxides upon contact with air (which are even more explosive). Do not use any ether that is older than 1 year (it should be disposed of safely). When removing ether (ie by rotavap) you must add a little hexane or some other solvent to your flask when the evaporation is nearing completion (because evaporation of ether concentrates the explosive peroxides). Never rotavap ether to completion when it is the sole solvent.

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14y ago

Ether is highly flammable, use it with caution (ie, use only in the fume hood, make sure there are no open flames in the vicinity, etc.). Ether has a flashpoint well below that of room temperature, meaning its vapor can easily catch fire or explode if you are not careful. Also, ether tends to form peroxides if left for a long period of time, which become explosive when concentrated (since these peroxides have a higher boiling point than that of ether). When removing your solvent after extraction, never evaporate ether to dryness. Always add some hexane near the end of the evaporation to co-evap any possible peroxides.

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14y ago

Some reactions produce both nonpolar products and nonpolar sideproducts. If the product precipitates in ether (because of its poor solubility) and the side products are not, then the ether can be added to the product-sideproduct mixture and filtered out. The solid product filtered out will be saved and the rest (the ether and side products) tossed out.

If the product is soluble in ether and the side-products are not, then the solid that is filtered would be tossed out and the ether and the desired product it contains will be kept. Purification of the product could be done by evaporating the volatile ether under a fume hood.

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16y ago

include low operating temperature and the ability to analyze the reaction with less volatile components

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9y ago

There are several disadvantages to using ether as a solvent. Some of those disadvantages are that ether is highly flammable, it can oxidize into an explosive and it is an anesthetic.

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12y ago

it offers easy recovery of extracts since ether has low boiling points it evaporates easily leaving behind the extracted solute

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Q: What are the adavantages of using ether as an extraction solvent?
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Advantages of using ether as an extracting solvent?

Some reactions produce both nonpolar products and nonpolar sideproducts. If the product precipitates in ether (because of its poor solubility) and the side products are not, then the ether can be added to the product-sideproduct mixture and filtered out. The solid product filtered out will be saved and the rest (the ether and side products) tossed out. If the product is soluble in ether and the side-products are not, then the solid that is filtered would be tossed out and the ether and the desired product it contains will be kept. Purification of the product could be done by evaporating the volatile ether under a fume hood.


What would happen to the isolation process if you use a more polar solvent such as methatnol inteasd of dietyl ether?

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