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What does cold filtration mean?

Updated: 4/28/2022
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12y ago

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it is where you separate a solid from a liquid using a funnel & filter paper

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Q: What does cold filtration mean?
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Why do you need to carry out two types of filterations to achieve purification of solids in recrystallization work?

The compound that you are trying to recrystallize is soluble in hot solvent but relatively insoluble in cold solvent. You also must remove an impurity that is insoluble in hot and cold solvent. The first filtration (a hot filtration) is to filter out the impurity. The second filtration (a cold filtration) is to filter out the (hopefully pure) recrystallized compound.


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Vacuum filtration is used instead of gravity filtration in order to achieve a dryer product in less time. The faster process of vacuum filtration allows the slurry to remain cold and in cases such as with benzoic acid more crytals will remain formed at colder temperatures. Gravity filtration is most useful when the solid is to be discarded and the filtrate (the liquid that flows through the filter paper) kept. Vacuum filtration is often faster than gravity filtration and is most useful if the solid must be kept or if a filtration must be done rapidly. A vacuum from an aspirator or a vacuum pump is used to pull the liquid through a funnel containing a piece of filter paper, while the solid is left on the paper.


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