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What is difference between open reflux and closed reflux chemical oxygen demand measurement?
Wiki User
∙ 12y ago
The closed reflux method is more efficient in the oxidation of volatile organic compounds than is the opened reflux method. The reason for this is that the oxidant is in contact with these compounds for a longer time. Besides, the closed method is cheaper as only 2 mL of sample is required, since 5 mL is the total volume of the mixture. This means that the amounts of reagents and sample are reduced by a factor of over 20 compared to the opened reflux method. In addition, this fact makes the method less contaminating and allows for the simultaneous digestion of a great number of samples
Wiki User
∙ 12y ago
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