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It would all depend entirely on the situation and environment that this experiment is conducted within. I'll try to cover the basic scenarios

Iron and Sulphur will not bond at regular boiling point. That being said, I will assume that these agents have not indeed bonded and are a mixture of the two minerals.

That being the case, you can separate Iron from Sulphur using a magnet.

Hope this answers your question

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Q: After heating iron and sulfur is it possible to use a magnet to separate the mixture?
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