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distillation separation
Effect of heat would be the solvent will be dissolved fast and the temperature changes contribute to the change of the effect of the supersaturated solution.
Ammonia would be the solute and water would be the solvent.
The solute would be iodine, and the solvent would be tincture
Water vapor would be the solvent. Water alone is a good solvent.
If a substance is dissolved in a solvent, distillation allows recovery of both the solvent and the solute.
If the original spots were below the level of developing solvent then the components of the spotted sample would dissolve into the solvent and no spots would be seen upon analysis because all of the sample is dissolved in the developing solvent. hope this helps. good luck in o. chem!
Distillation separation
If the solvent level in the developing jar is deeper than the origin (spotting line) of the TLC plate, the solvent will dissolve the compounds into the solvent reservoir instead of allowing them to move up the plate by capillary action. Thus, you will not see spots after the plate is developed. These photos show how the yellow compound is running into the solvent when lifted from the developing jar.
distillation separation
In choosing solvent i would consider the following factors: What are the solutes? - are they polar or nonpolar how should they be dissolved What is the next step? - E.G. Do you need to distil or heat, then boiling point would be important. Is the solvent inert? Obviously side reactions are bad so choose a solvent which will not react. Good solvents are ethyl ether or ethyl alcohol.
Effect of heat would be the solvent will be dissolved fast and the temperature changes contribute to the change of the effect of the supersaturated solution.
By placing the spot above the level of the solvent in the beaker, you slow the flow of solvent which results in improved separation of the components in the spot. If you placed it below the level of the solvent in the beaker, the solvent would just flow at a much faster rate and instead of separating the components in the spot, they would simply be washed away.
The solute would be iodine, and the solvent would be tincture
You would recrystallize a solid from a solvent pair because if only one solvent was used, then it might be hard to dissolve the solute. In a solvent pair, one solvent would probably be better at dissolving the solute.
The solvent would be water, the solute would be the chlorine chemicals
Ammonia would be the solute and water would be the solvent.