yes
Acetanilide
The amide group on acetanilide is an ortho/para director, so a simple nitration should work: a mixture of sulfiric acid and nitric acid should be sufficient. Afterward, separation of the ortho and para compounds (by column chromatography, probably) would be necessary.
p-nitro phenol has a symmetric structure as compare to o-nitro phenol so it has higher dipole moment or polarity so is more soluble.
243.5 nm in 0.1 N Hydrochloric acid
used of para nitro acet anilide
Why is not acetanilide soluble in HCL?
An acetanilide is an amide derived from acetic acid and aniline, once used as an analgesic and antipyretic.
the most suitable for recrystrallizing acetanilide is water..
Yes. Heptane is an ideal recrystallization solvent for acetanilide.
In the synthesis of acetanilide the hydrochloride salt of aniline is used in order to increase the solubility in water. The sodium acetate acts as a base and reacts with the HCl to produce acetic acid. Once the acetanilide product is no longer a hydrochloride salt, its solubility in water is decreased and it crystalises out. The main byproducts are sodium chloride and acetic acid which remain soluble in the water and are removed when the crude product is filtered off.
yes
Acetanilide is a substituted aromatic amide insoluble in water and is almost neutral so does not react with litmus.
HNO3 + H2SO4 acts as a sulphonating agent. It reacts with acetanilide to from 4-Acetylamino-benzenesulfonic acid.
It is most useful when crystals are being filtered out of a desired product. Why is water a good solvent for the recrystallization of acetanilide? Acetanilide readily dissolves in hot water, but is insoluble at low temps. Thus, it dissolves in hot water but crystalizes easily when cool.
Terrible technique
acetanilide results in the deactivation of the heamoglobin in some red blood cells. This means they can uptake fewer oxygen molecules therefore you may feel breathless, tired ect