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What is sulphated ash?

Updated: 4/28/2022
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13y ago

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The sulphated ash test is an analytical test for determining the inorganic content of a sample by weight. The sample ( usually 1g) is accurately weighed into a platinum, silica crucible that has been previously ignited, cooled and weighed. The sample in the crucible is then subjected to sulphuric acid (usually 1mL) and charred at a low temperature without causing ignition of the sample until there are no more white fumes given off. The crucible with the charred sample is then placed in a furnace (temperature is dependent on monograph but typically it can be from 600 to 900 degrees celcius) until all organic matter has been burnt off. The crucible is cooled and re-weighed. The difference in sample weights being the sulphated ash content remaining. Some monographs require the sample to be re-ashed until a constand weight has been achieved. The remaining inorganic matter is typically metal oxides from most samples.

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Q: What is sulphated ash?
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The only difference between sulphated ash and the residue on ignition is the terminology. The residue on an ignition is sulphated ash.


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