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Start with 1 dm^3 (1 Liter) of pure H2O. Molarity is defined as Mol/dm^3, so this is generally an easy way to go.

Measure out 3 mol of H2SO4 -> First find the molar weight of Sulfuric acid, which is, according to Google: 98.079g/mol.

So 3 mol * 98.079g/mol = 294.24 grams of H2SO4.

Add that to 1 Liter of water, and you'll have an aqueous 3 Molar solution!

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