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If you need to make just 100mL, then you need 1 tenth of a liter that is 5M. If you were to make 1L of 5 molar NaCl, you would need 5 times the molar mass of NaCl (58.44g/mol) dissolved in 1L of water. Thus for 1L of a 5M solution you need 5 * 58.44g, or 292.2 grams of NaCl.

However, since we only want 100mL, which is 1/10 of a Liter, we also only need 1/10 the amount of NaCl, or 292.2 / 10, which is 29.22g.

So, measure out 29.22g NaCl, and dissolve completly in a volume less than 100mL, say 80mL, then bring the final volume up to 100mL.

You now have 100mL of a 5M NaCl solution.

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